Scrape the cells in the presence of PBS or cold (+4°C) saline serum.
Transfer them in a conical tube.
Centrifuge at 1500 rpm/5 minutes.
Gently aspirate as much supernatant as possible in order to obtain the driest possible pellet.
Place the tube in ice
Freeze the tube as soon as possible. (if possible transfer to – 80°C as quickly as possible).
Blood cell samples
Draw two 5 mL EDTA tubes or vacutainers.
Red blood cells and plasma
Use one 5 mL EDTA tube
Centrifuge at + 4 °C (if possible) at approx. 3000 rpm for 10 minutes.
Separate the plasma: separate into three aliquots of 500 µL each.
Wash the pellets of the globules with saline + 4 °C (0.9% NaCl), volume to volume.
Shake by inversion
Centrifuge at approx. 3000 rpm, + 4 °C if possible, 5 minutes.
Remove supernatants by aspirating the interface of white blood cells and platelets (e.g. using soft plastic pipettes).
Repeat the washing operation once.
Divide into 3 fractions, > 100 microliters each
Freeze plasma and cell fractions at – 20 °C as quickly as possible (if possible transfer quickly to – 80°C).
White blood cells, lymphocytes
Use the second 5 mL EDTA tube
Dilute a volume of blood with the same volume of NaCl 0.9%, (1V/1V)
Pour diluted blood over 1V of lymphoprep®. Pay attention to the deposit. It must be performed as gently as possible, inverting the drops, drop by drop for the first mL, on the wall of the tube, as close as possible to lymphoprep®. There should be no mixing between diluted blood and lymphoprep®. This is an important prerequisite for the success of the subsequent separation.
Centrifuge 4000 rpm 20min at 20°C (avoid cold centrifuge)
Remove diluted plasma
Pipette (white) lymphocytes layer.
Transfer to an eppendorf tube
Wash the cells with at least 1 mL saline + 4 °C (0.9% NaCl).
Shake by inversion
Centrifuge at approx. 3000 rpm, + 4 °C if possible, 5 minutes.
Remove as much supernatant as possible with a pipette, in order to have as little residual volume as possible.
Freeze as quickly as possible at -20°C (if possible quickly transfer to – 80°C).
Tissue specimen collection
Biopsies should be frozen as soon as possible.
Punch biopsy
Place it as soon as possible in a freezer tube (NUNC tube) for liquid nitrogen.
Dispose of this tube in liquid nitrogen (thermos tanks).
Transfer the tube to the freezer (if possible transfer quickly to – 80°C).
Specimen transfer
Transport specimen in dry ice or any other means that ensures a temperature below – 10°C.